Wc. Jeong et al., OBSERVATION OF DEFORMATION AND TRANSFORMATION BEHAVIOR OF RETAINED AUSTENITE IN A 0.14C-1.2SI-1.5MN STEEL WITH FERRITE BAINITE AUSTENITE STRUCTURE, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 165(1), 1993, pp. 1-8
A 0.14wt.%C-1.21wt.%Si-1.57wt.%Mn steel was intercritically annealed a
t 770-degrees-C for 5 min and then isothermally held at 400-degrees-C
for 4 min followed by oil quenching to room temperature. The as-anneal
ed microstructure consisted of 75% ferrite, 13% bainite, and 12% retai
ned austenite. The steel was used to establish a microscopic method to
identify retained austenite, and to observe the deformation and trans
formation behavior of the retained austenite with tensile deformation.
Submicron-sized particles of retained austenite could be distinguishe
d from ferrite, bainite and martensite in light microscopy when etched
with 5% nital followed by etching in a 10% sodium metabisulphite solu
tion. The retained austenite particles were observed in three types of
locations: type I at ferrite grain boundaries always in contact with
bainite; type II at ferrite grain boundaries out of contact with baini
te; and type III within ferrite grains. It was also observed that the
larger retained-austenite particles transformed more easily to martens
ite during deformation at room temperature. Even after deformation to
a tensile strain greater than 32%, about 4% of the retained austenite
remained, and the retained-austenite particles were observed in the de
formed structure.