P. Ancrenaz et al., SMALL-ANGLE X-RAY-SCATTERING STUDY OF PRECIPITATION IN A CU-2 AT-PERCENT CO ALLOY, Acta crystallographica. Section B, Structural science, 49, 1993, pp. 458-463
The unmixing at 923 K of a binary alloy Cu-2 at.% Co was studied by an
omalous small-angle X-ray scattering performed at the CoK-absorption e
dge and transmission electron microscopy. For ageings of 3 and 120 h a
marked anomalous effect was observed. Experimental curves were fitted
with the help of a model that took into account the radius of precipi
tates, their volume fraction and the radius of excluded spheres. X-ray
absolute scattered-intensity measurements allowed us to determine the
cobalt concentration in precipitates.