SMALL-ANGLE X-RAY-SCATTERING STUDY OF PRECIPITATION IN A CU-2 AT-PERCENT CO ALLOY

Citation
P. Ancrenaz et al., SMALL-ANGLE X-RAY-SCATTERING STUDY OF PRECIPITATION IN A CU-2 AT-PERCENT CO ALLOY, Acta crystallographica. Section B, Structural science, 49, 1993, pp. 458-463
Citations number
9
Categorie Soggetti
Crystallography
ISSN journal
01087681
Volume
49
Year of publication
1993
Part
3
Pages
458 - 463
Database
ISI
SICI code
0108-7681(1993)49:<458:SXSOPI>2.0.ZU;2-L
Abstract
The unmixing at 923 K of a binary alloy Cu-2 at.% Co was studied by an omalous small-angle X-ray scattering performed at the CoK-absorption e dge and transmission electron microscopy. For ageings of 3 and 120 h a marked anomalous effect was observed. Experimental curves were fitted with the help of a model that took into account the radius of precipi tates, their volume fraction and the radius of excluded spheres. X-ray absolute scattered-intensity measurements allowed us to determine the cobalt concentration in precipitates.