N. Ikarashi et al., HIGH-RESOLUTION TRANSMISSION ELECTRON-MICROSCOPY OF ALAS GAAS INTERFACIAL STRUCTURE IN THE 110 PROJECTION/, JPN J A P 1, 32(6A), 1993, pp. 2824-2831
We have established an imaging condition of [110] high-resolution tran
smission electron microscopy (HREM) for edge-on observations of AlAs/G
aAs interfacial step structures. It is shown that [110] HREM images of
GaAs and AlAs show a remarkable contrast around a specimen thickness
equivalent to the GaAs extinction distance due to a large difference i
n {111} amplitudes between GaAs and AlAs. A specimen preparation techn
ique in which chemical etching was used to remove ion milling artifact
s was also developed to accomplish this observation. Using this HREM m
ethod, we have made observations of AlAs/GaAs interfaces grown by mole
cular beam epitaxy, giving information about the straightness of the i
nterfacial step edges and the distribution of step intervals. These re
sults show a marked difference in the interfacial step structure betwe
en steps parallel to [110BAR] and steps parallel to [110].