IDENTIFICATION OF SOLID-SOLUTIONS OF COPRECIPITATED NI-CO OXALATES USING XRD, TG AND SEM TECHNIQUES

Authors
GAO X CHEN D DOLLIMORE D SKRZYPCZAKJANKUN E BURCKEL P
Citation
X. Gao et al., IDENTIFICATION OF SOLID-SOLUTIONS OF COPRECIPITATED NI-CO OXALATES USING XRD, TG AND SEM TECHNIQUES, Thermochimica acta, 220, 1993, pp. 75-89
Citations number
14
Categorie Soggetti
Chemistry Analytical
Journal title
Thermochimica acta → ACNP
ISSN journal
00406031
Volume
220
Year of publication
1993
Pages
75 - 89
Database
ISI
SICI code
0040-6031(1993)220:<75:IOSOCN>2.0.ZU;2-R
Abstract
Homogeneous solid-solution oxalates of Ni2+ and Co2+ ions were synthes ized by coprecipitation from nitrate solutions using a double-inlet te chnique. The identification of the solid solutions used X-ray powder d iffraction (XRD), thermogravimetry (TG) and scanning electron microsco py (SEM) techniques. The experimental results showed that the coprecip itated powders have characteristics that are different from those of t he mechanical mixtures with the same stoichiometry.