Cw. Lawrence et al., ACOUSTIC MICROSCOPY OF CERAMIC-FIBER COMPOSITES .2. METAL-MATRIX COMPOSITES, Journal of Materials Science, 28(13), 1993, pp. 3653-3660
Scanning acoustic microscopy (SAM) has been used to study metal matrix
composites (MMCs) reinforced with silicon-carbide monofilaments, For
most of the specimens the matrix was Ti-6Al-4V, but Ti3Al and 6061 Al
matrices were also examined. The titanium-matrix specimens were subjec
ted to a range of thermal ageing treatments to investigate potential i
n-service degradation. The main effect was progressive deterioration o
f the fibre-matrix interface. In the as-received material the carbon-r
ich coating protected the SiC by forming a reaction layer with the tit
anium. As a result of ageing, the reaction layer was penetrated adjace
nt to the beta-phase titanium grains. More extensive ageing caused the
carbon-rich coating to degrade and eventually disappear. The final st
age of deterioration was direct attack on the SiC. Cracks and porosity
between fibres were observed in some specimens, probably due to poor
diffusion bonding during fabrication. Fine radial microcracks were obs
erved in an annular region inside the mid-radius of some fibres; they
are believed to be a consequence of stress relief during thermal agein
g. These cracks could not be observed optically. The extra sensitivity
of acoustic microscopy is due to the reflection of Rayleigh waves by
tight closed cracks.