A FACILE SYNTHESIS OF ALDEHYDE AND KETONE VIA SONOCHEMICAL BARBIER REACTION AND OXIDATION

Authors
LEE ASY KUNG CC
Citation
Asy. Lee et Cc. Kung, A FACILE SYNTHESIS OF ALDEHYDE AND KETONE VIA SONOCHEMICAL BARBIER REACTION AND OXIDATION, Journal of the Chinese Chemical Society, 44(1), 1997, pp. 65-69
Citations number
26
Categorie Soggetti
Chemistry
Journal title
Journal of the Chinese Chemical Society → ACNP
ISSN journal
00094536
Volume
44
Issue
1
Year of publication
1997
Pages
65 - 69
Database
ISI
SICI code
0009-4536(1997)44:1<65:AFSOAA>2.0.ZU;2-R
Abstract
Methyl ketone is prepared by a sonochemical Barbier reaction of methyl iodide, magnesium powder and aldehyde in Benzene/THF (9/1) solvent in a commercial ultrasonic cleaning bath (39 kHz), followed by the addit ion of N-chlorosuccinimide (NCS) as an oxidizing agent.