SUPERCRITICAL-FLUID EXTRACTION AND CHROMATOGRAPHY MASS-SPECTROMETRY OF FLAME RETARDANTS FROM POLYURETHANE FOAMS

Authors
MACKAY GA SMITH RM
Citation
Ga. Mackay et Rm. Smith, SUPERCRITICAL-FLUID EXTRACTION AND CHROMATOGRAPHY MASS-SPECTROMETRY OF FLAME RETARDANTS FROM POLYURETHANE FOAMS, Analyst, 118(7), 1993, pp. 741-745
Citations number
17
Categorie Soggetti
Chemistry Analytical
Journal title
Analyst → ACNP
ISSN journal
00032654
Volume
118
Issue
7
Year of publication
1993
Pages
741 - 745
Database
ISI
SICI code
0003-2654(1993)118:7<741:SEACMO>2.0.ZU;2-W
Abstract
Four chlorinated organophosphate flame retardants present in polyureth ane foams were analysed by supercritical fluid chromatography with fla me-ionization detection and mass spectrometry. In addition, their amen ability to gas chromatography was investigated. Real samples were anal ysed by using these techniques after on-line extraction with supercrit ical carbon dioxide. On-line quantitative extraction of the flame reta rdants from the polyurethane foams was investigated by using an extern al calibration.