DETERMINATION OF TOTAL OIL IN PETROLEUM TANKER BALLAST WATER BY ZEROTH-DERIVATIVE, 1ST-DERIVATIVE AND 2ND-DERIVATIVE INFRARED SPECTROPHOTOMETRY AND LEAST-SQUARES CURVE-FITTING

Citation
Pp. Losada et al., DETERMINATION OF TOTAL OIL IN PETROLEUM TANKER BALLAST WATER BY ZEROTH-DERIVATIVE, 1ST-DERIVATIVE AND 2ND-DERIVATIVE INFRARED SPECTROPHOTOMETRY AND LEAST-SQUARES CURVE-FITTING, Vibrational spectroscopy, 5(2), 1993, pp. 245-251
Citations number
21
Categorie Soggetti
Spectroscopy,"Chemistry Analytical","Chemistry Physical
Journal title
ISSN journal
09242031
Volume
5
Issue
2
Year of publication
1993
Pages
245 - 251
Database
ISI
SICI code
0924-2031(1993)5:2<245:DOTOIP>2.0.ZU;2-Q
Abstract
A rapid method for the determination of total hydrocarbons in random s amples of oil tanker ballast water is described. A 1-l sample is treat ed with CCl4 after acidification with HCl. The organic extract is anal ysed by measuring features in the zeroth-, first- and second-derivativ e infrared spectra using the Perkin-Elmer SNGLE program and by means o f least-squares curve-fitting algorithms of the zeroth- or first-deriv ative IR spectra using the Perkin-Elmer QUEST program.