V. Sachan et Jd. Meakin, STUDY OF PHASES FORMED DURING PRODUCTION OF COPPER INDIUM DISELENIDE BY REACTING COPPER, INDIUM AND SELENIUM LAYERS, Solar energy materials and solar cells, 30(2), 1993, pp. 147-160
CuInSe2 films were grown by reacting stacked layers of Cu, In and Se i
n an atmosphere of Se vapor. Incremental growth of the various phases
was followed at different temperatures until a single phase CuInSe2 fi
lm Was formed. Conventional X-ray diffraction was used in identifying
the different phases formed. Along with the knowledge of different pha
ses formed at increasing reaction temperatures, it was concluded that
CuInSe2 is formed at temperatures as low as 235-degrees-C, although a
single phase film is obtained only at higher temperatures (almost-equa
l-to 350-degrees-C).