NITROARENES IN AIRBORNE PARTICULATE ORGANIC EXTRACTS COLLECTED FROM UPPER SILESIA - IDENTIFICATION AND QUANTITATIVE-ANALYSIS

Authors
Citation
L. Warzecha, NITROARENES IN AIRBORNE PARTICULATE ORGANIC EXTRACTS COLLECTED FROM UPPER SILESIA - IDENTIFICATION AND QUANTITATIVE-ANALYSIS, Chemia Analityczna, 38(3), 1993, pp. 303-313
Citations number
19
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00092223
Volume
38
Issue
3
Year of publication
1993
Pages
303 - 313
Database
ISI
SICI code
0009-2223(1993)38:3<303:NIAPOE>2.0.ZU;2-H
Abstract
The silicic acid column chromatography was employed to isolate the nit roarene fraction from the dichloromethane extracts of airborne particu late matter collected in twelve places in Upper Silesia region. The se lective isolation of nitroarenes from PAH and carbazoles was acquired by means of converting nitrocompounds into pentafluoropropylamides. Th e use GC-MS system and capillary GC in the analysis of amides made it possible to identify nitrofluorene, nitropyrene, nitrofluoranthene in the most of analysed samples. It also helped to make the quantitative determination of these compounds.