This paper presents the extraction of nickel using nitric acid from wa
ste nickel catalyst used in hydrogenation of oils and fats. The compou
nds of sulphur, phosphorus, nitrogen, etc., poisoning agents of cataly
st and other acid insoluble fractions, are removed in order to utilize
the waste catalyst. The extraction process has been optimized. It has
been observed that countercurrent extraction up to three-stage with t
hree normal acid and one hour duration are the best process conditions
.