A NEW SYNTHETIC ROUTE TO 2-(P-NITROBENZYL)-1,4,7,10-TETRAAZACYCLODODECANE

Authors
GARRITY ML BROWN GM ELBERT JE SACHLEBEN RA
Citation
Ml. Garrity et al., A NEW SYNTHETIC ROUTE TO 2-(P-NITROBENZYL)-1,4,7,10-TETRAAZACYCLODODECANE, Tetrahedron letters, 34(35), 1993, pp. 5531-5534
Citations number
11
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron letters → ACNP
ISSN journal
00404039
Volume
34
Issue
35
Year of publication
1993
Pages
5531 - 5534
Database
ISI
SICI code
0040-4039(1993)34:35<5531:ANSRT2>2.0.ZU;2-W
Abstract
A new, general synthetic method for the title compound has been develo ped, based on the nitration of 2-benzyl-1,4-7,10-tetraazacyclododecane (64 % yield), which provides higher yields and easier purification fo r scale-up than previously reported methods.