Y. Hirata et K. Takeshima, COLLOIDAL PROCESSING FOR LAMINATED COMPOSITES OF MULLITE ALUMINA WOVEN FABRICS, Materials letters, 17(3-4), 1993, pp. 125-130
A sol-gel-processed mullite powder and alumina woven fabrics were for-
med into laminated composites (5 vol% alumina fabrics) by filtration o
f the aqueous mullite suspensions containing polyacrylic ammonium at p
H = 8.8 which were poured into the spaces separated with alumina fabri
cs. The mullite suspensions with 30-55 vol% solids showed a Newtonian
flow and formed high-density green compacts of 60-63% of the theoretic
al density (TD). The green composites were densified to near full dens
ity by hot-pressing at 1650-degrees-C for 1 h at 39 MPa in N2 atmosphe
re. The mechanical properties (strength, hardness and fracture toughne
ss) of the dense composites (> 99% TD) were measured at room temperatu
re. However, no significant improvements of strength and fracture toug
hness were obtained due to the formation of large cracks (> 100 mum) a
cross the alumina fabrics and disappearance of long fiber characterist
ics after sintering.