SEMIPREPARATIVE SYNTHESIS, C-13-NMR AND 2D-NMR OF PULOUPONE

Authors
MATIKAINEN J KALTIA S HASE T KILPELAINEN I DRAKENBERG T ANNILA A
Citation
J. Matikainen et al., SEMIPREPARATIVE SYNTHESIS, C-13-NMR AND 2D-NMR OF PULOUPONE, Tetrahedron, 49(36), 1993, pp. 8007-8014
Citations number
17
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron → ACNP
ISSN journal
00404020
Volume
49
Issue
36
Year of publication
1993
Pages
8007 - 8014
Database
ISI
SICI code
0040-4020(1993)49:36<8007:SSCA2O>2.0.ZU;2-R
Abstract
A mmolar scale synthetic route to (+/-)-pulo'upone, in 9 steps, 3.8% o verall yield, and under non-epimerizing conditions, is reported. A com plete assignment of the compound's H-1 and C-13 NMR shifts is presente d.