G. Pezzotti et al., A QUANTITATIVE-EVALUATION OF MICROSTRUCTURE IN SI3N4 SIC PLATELET ANDPARTICULATE COMPOSITES/, Journal of Materials Science, 28(17), 1993, pp. 4787-4798
A microstructural evaluation of Si3N4 containing 15-40 vol% SiC platel
ets or particles is presented. All the composites were fully densified
by hot isostatic pressing without external addition of sintering aids
. Size, morphology, surface roughness and crystal structures of the Si
C phases before and after sintering were compared in order to discuss
the structural stability of the reinforcements up to 2050-degrees-C in
Si3N4 matrix. Morphology and phase characteristics of the grain bound
ary are also discussed. In addition, homogeneity and isotropy of the c
omposite bodies were quantitatively examined by image analysis techniq
ues and it was recognized that, for a similar degree of dispersion, th
e characteristic of three-dimensional randomness could be preserved on
ly at V(f) < 30% in the composites containing high aspect ratio platel
ets.