X-RAY STRUCTURAL CHARACTERIZATION OF DICYCLOHEXYLAMMONIUM CHLORIDE AND ITS CONVERSION TO BROMOFLUOROPHOSPHATE, IODOFLUOROPHOSPHATE AND HEXAFLUOROPHOSPHATE DERIVATIVES
J. Gopalakrishnan et al., X-RAY STRUCTURAL CHARACTERIZATION OF DICYCLOHEXYLAMMONIUM CHLORIDE AND ITS CONVERSION TO BROMOFLUOROPHOSPHATE, IODOFLUOROPHOSPHATE AND HEXAFLUOROPHOSPHATE DERIVATIVES, Indian journal of chemistry. Sect. B: organic chemistry, including medical chemistry, 36(1), 1997, pp. 47-49
Single crystal X-ray structural determination of dicyclohexylammonium
chloride, prepared easily in quantitative yield by a modified procedur
e, reveals it to be strongly and intermolecularly hydrogen bonded. Whi
le its bromide derivative is readily obtained in nearly quantitative y
ield, the iodide and hexafluorophosphate salts are formed slowly in mo
derate yields.