X-RAY STRUCTURAL CHARACTERIZATION OF DICYCLOHEXYLAMMONIUM CHLORIDE AND ITS CONVERSION TO BROMOFLUOROPHOSPHATE, IODOFLUOROPHOSPHATE AND HEXAFLUOROPHOSPHATE DERIVATIVES

Citation
J. Gopalakrishnan et al., X-RAY STRUCTURAL CHARACTERIZATION OF DICYCLOHEXYLAMMONIUM CHLORIDE AND ITS CONVERSION TO BROMOFLUOROPHOSPHATE, IODOFLUOROPHOSPHATE AND HEXAFLUOROPHOSPHATE DERIVATIVES, Indian journal of chemistry. Sect. B: organic chemistry, including medical chemistry, 36(1), 1997, pp. 47-49
Citations number
13
Categorie Soggetti
Chemistry Inorganic & Nuclear
ISSN journal
03764699
Volume
36
Issue
1
Year of publication
1997
Pages
47 - 49
Database
ISI
SICI code
0376-4699(1997)36:1<47:XSCODC>2.0.ZU;2-6
Abstract
Single crystal X-ray structural determination of dicyclohexylammonium chloride, prepared easily in quantitative yield by a modified procedur e, reveals it to be strongly and intermolecularly hydrogen bonded. Whi le its bromide derivative is readily obtained in nearly quantitative y ield, the iodide and hexafluorophosphate salts are formed slowly in mo derate yields.