DETERMINATION OF PESTICIDES IN RIVER WATER BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY SELECTED-ION MONITORING

Authors
KOBAYASHI H OHYAMA K TOMIYAMA N JIMBO Y MATANO O GOTO S
Citation
H. Kobayashi et al., DETERMINATION OF PESTICIDES IN RIVER WATER BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY SELECTED-ION MONITORING, Journal of chromatography, 643(1-2), 1993, pp. 197-202
Citations number
8
Categorie Soggetti
Chemistry Analytical
Journal title
Journal of chromatography → ACNP
Volume
643
Issue
1-2
Year of publication
1993
Pages
197 - 202
Database
ISI
SICI code
Abstract
A highly sensitive and specific method for the determination of trace levels of pesticides in river water has been developed. The method is based on reversed-phase (C18) solid phase extraction, followed by gas chromatography-mass spectrometry-selected-ion monitoring. Recoveries a t the 0.5- or 2.5 mug/l fortification level were between 79 and 98%. T he detection limits were 0.05 mug/l for chlornitrofen and 0.01 mug/l f or other pesticides.