Sulphate-based magnesium-zinc-aluminium synthetic hydrotalcite-like co
mpounds have been prepared by coprecipitation with a sodium hydroxide
solution. The corresponding metal solutions were coprecipitated at pH
10, aged in the mother liquor, washed several times and dried at 40-de
grees-C. Whatever the ratio of metal ions in the initial metal sulphat
e solutions, hydrotalcite compounds were formed during coprecipitation
. The temperature of preparation and ageing time did not effect the fi
nal crystal structure. By comparing the properties of the Mg-Al layere
d compounds, it seems that when the zinc content increases, the therma
l stability of the hydrotalcite-like compounds decreases.