A. Schumacher et al., SINGLE-LAYER MOS2 ON MICA - STUDIES BY MEANS OF SCANNING FORCE MICROSCOPY, Surface science, 289(1-2), 1993, pp. 120000595-120000598
Molecular layers of molybdenum disulfide on mica were studied by scann
ing force microscopy (SFM). The measured unit cell dimensions, 0.32 an
d 0.52 mm, are consistent with the bulk structures of both MoS2 and mi
ca, respectively. This is the first example of a study with atomic res
olution of two chemically different materials obtained in one and the
same SFM image. The MoS2 layer height was found to be 1.3 +/- 0.3 nm a
nd was interpreted as being due to the presence of single-layers with
variable amounts of water adsorbed on either side and on the mica surf
ace. Furthermore, the occurrence of friction effects between the sampl
e and the probing tip is considered to influence the layer height dete
rmination.