Magnetic properties of equiatomic FeCu alloys, obtained by mechanical
alloying, were measured in a temperature range between 5 and 300K. The
as-milled sample consists of a metastable fcc FeCu phase with a tempe
rature dependence of magnetization which follows a T3/2 law. This meta
stable phase decomposes into Cu and Fe phases with annealing. After an
nealing at 820K, the magnetization value at low temperature is 30% sma
ller than the unannealed state. The Mossbauer spectrum obtained at roo
m temperature shows a paramagnetic Fe phase with a relative resonant a
rea of 30%. These results suggest that after this annealing process 30
% of the iron is not in the ferromagnetic alpha phase but in a non-mag
netic state (with vanishing atomic magnetic moment) or probably formin
g an antiferromagnetic gamma-Fe phase (which is paramagnetic at room t
emperature).