Mq. Ding et al., PREPARATION AND CHARACTERIZATION OF YBA2CU3O7-X HIGH-TC SUPERCONDUCTING THIN-FILMS DEPOSITED BY S-GUN SPUTTERING, Thin solid films, 230(2), 1993, pp. 179-182
We have prepared YBa2Cu3O7-x high T(c) superconducting (HTS) thin film
s on (100) yttria-stabilized zirconia (YSZ) and LaAlO3 (LAO) substrate
s, using a 2 kW S-gun in an off-axis mode. By varying the temperature
of the substrates, films with a axis and c axis orientations were read
ily obtained. The X-ray diffraction pattern and Laue pattern confirmed
that films with a axis orientation exhibited a single-crystal texture
. All films had a good mirror-like surface. For films grown on YSZ sub
strates, scanning electron microscopy (SEM) revealed a clear distincti
on between the surfaces of the films grown at various temperatures (52
0-780-degrees-C). Films grown on LAO substrates exhibited even smoothe
r and flatter surfaces. The SEM changes will be discussed in correlati
on with J(c). The best HTS thin films were obtained on LAO substrates
at a temperature of 820-degrees-C, with T(c) = 89 K and J(c) = 1 x 10(
6) A cm-2 (77 K).