Mr. Schock et Gk. George, EVALUATION OF A FIELD-TEST KIT FOR MONITORING LEAD IN DRINKING-WATER, Journal - American Water Works Association, 85(8), 1993, pp. 90-100
This article describes a conceptual framework for designing evaluation
studies of test kits for the analysis of significant drinking water c
onstituents. A commercial test kit for the analysis of lead in tap wat
ers was evaluated and compared with a standard graphite furnace atomic
absorption spectrophotometry (GFAAS) technique. The kit was relativel
y free of operator bias and had a detection limit of 4 mug/L in spiked
deionized water. Above the detection limit of the kit, accuracy was c
omparable to that of GFAAS when samples were analyzed in triplicate. T
he relative precision of the kit varied with concentration. The absolu
te precision of the kit was about +/-3 mug/L from 10 to 100 mug/L. Sig
nificant interferences were found for certain concentration thresholds
of zinc, iron [Fe(II)], polyphosphate species, and orthophosphate. Hi
gh concentrations of aluminum and chloride reduced method precision. S
everal operational changes are presented that improve precision and ac
curacy of the test kit for field and laboratory use.