THERMALLY STIMULATED CURRENT STUDY OF THE MOLECULAR-MOVEMENTS IN BONE

Citation
M. Mourgues et al., THERMALLY STIMULATED CURRENT STUDY OF THE MOLECULAR-MOVEMENTS IN BONE, Journal of thermal analysis, 40(2), 1993, pp. 863-869
Citations number
5
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
03684466
Volume
40
Issue
2
Year of publication
1993
Pages
863 - 869
Database
ISI
SICI code
0368-4466(1993)40:2<863:TSCSOT>2.0.ZU;2-L
Abstract
Thermally Stimulated Current (TSC) has been used for investigating the interface and interphase in a natural composite, bone. Young adult ma le femoral diaphysis has been studied at different stages of demineral ization by EDTA. Analysis of the fine structure of complex TSC spectra has shown that in the early stages of demineralization, dielectric re laxations are due to the hydroxyl reorientations in the mineral apatit e structure. After a certain stage of demineralization, the mineral re sponse disappears and organic matrix mobility is observed. A dissociat ive buffer has been used to identify collagen relaxations. The contrib ution of the mineral-organic interface/interphase has been isolated.