Transient heat pulse techniques allow specific heat C and thermal cond
UCtiVity kappa to be determined from a single measurement. In the main
these parameters have previously been derived using linearizations of
simplified solutions to the diffusion equation in restricted time reg
imes. We present a numerical fitting technique which allows a fit to b
e made to the full solution of the diffusion equation across all times
of the measurement. This technique also accounts for and allows measu
rement of the boundary resistance at the clamped end of the sample, an
effect which can cause significant distortion of the measured tempera
ture profile. This distortion can lead to significant errors in values
of C and kappa derived using other methods.