Da. Lytle et al., INVESTIGATING THE PREFERENTIAL DISSOLUTION OF LEAD FROM SOLDER PARTICULATES, Journal - American Water Works Association, 85(7), 1993, pp. 104-110
During a building corrosion control study, bottles containing acid-pre
served water samples with high levels of lead often had particulate ma
terial on the bottom. Scanning electron microscope analysis of the par
ticles showed the presence of tin and the absence of lead, indicating
the probable source of lead to be lead-tin solder. A leaching study wa
s done to investigate the effectiveness of the standard 0.15 percent n
itric acid preservation procedure for dissolving lead corrosion by-pro
ducts. Results indicate that the technique was adequate for dissolving
lead from lead-tin solder particles but not for tin.