It is shown how light scattering provides a powerful tool for thin-fil
m characterization. The introduction of a roughness isotropy degree pe
rmits the extraction of structural parameters of the stacks. Replicati
on functions and residual roughnesses are given for TiO2, SiO2, and Ta
2O5 materials produced by ion-assisted deposition and ion plating. Add
itional confirmation is given by measurements of scattering versus wav
elength. The sensitivity of design to material and substrate effects i
s studied. At low-loss levels, surface and bulk phenomena are discusse
d together. Microstructure is characterized in the frequency bandwidth
given by experiment.