Dc. Slavik et al., DETERMINING FRACTURE FACET CRYSTALLOGRAPHY USING ELECTRON BACKSCATTERPATTERNS AND QUANTITATIVE TILT FRACTOGRAPHY, Journal of materials research, 8(10), 1993, pp. 2482-2491
A methodology is presented to characterize the crystallography of indi
vidual fracture surface facets. Electron backscatter patterns (EBSP's)
from a metallographic section through a facet identify grain orientat
ion, and quantitative tilt fractography identifies facet orientation;
these results are combined to establish fracture facet crystallography
. For this technique, facet electropolishing is not required, the face
t alignment procedure is accurate and quick, and the method can be gen
eralized to different microstructures, test environments, or facet ori
entations. Method accuracy is illustrated for 25 to 50 mum fatigue cra
ck facets in an unrecrystallized Al-Li-Cu alloy (AA2090) that has 5 mu
m thick subgrains in elongated grains that are 10 to 200 mum thick. Th
e fine subgrain structure and tortuous fatigue crack profile precludes
the use of other diffraction techniques for determining AA2090 facet
crystallography. EBSP and tilt fractography results demonstrate that v
acuum fatigue cracks in AA2090 are nearly parallel to local {111} plan
es.