Inhomogeneities of composition, microstructure, and critical currents in elongated melt-textured YBCO samples

Citation
Vv. Prisedskii et al., Inhomogeneities of composition, microstructure, and critical currents in elongated melt-textured YBCO samples, INORG MATER, 34(12), 1998, pp. 1247-1252
Citations number
12
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
INORGANIC MATERIALS
ISSN journal
00201685 → ACNP
Volume
34
Issue
12
Year of publication
1998
Pages
1247 - 1252
Database
ISI
SICI code
0020-1685(199812)34:12<1247:IOCMAC>2.0.ZU;2-U
Abstract
The microstructure, preferred orientation, and axial inhomogeneities of com position and critical currents in melt-textured YBCO samples in the shape o f bars were studied. The microstructure of the material is dominated by lar ge platelike grains. Most of these grains consist of YBa2Cu3Ox (123 phase); large grains of Y2BaCuO5 (211 phase) and a 123/211 intergrowth phase are a lso present. In addition, the material contains small, randomly oriented gr ains of Y2BaCuO5, YBa2Cu3Ox, and BaCuO2. A wide scatter in 211 content and oxygen stoichiometry of 123 along the bar samples is revealed. The variatio ns in phase composition are found to be strongly correlated with those in c ritical current.