Application of laser polarimetry to the measurement of the specific heat capacity of molybdenum in the range 2000 to 2800 K by a pulse-heating technique
A. Cezairliyan et al., Application of laser polarimetry to the measurement of the specific heat capacity of molybdenum in the range 2000 to 2800 K by a pulse-heating technique, INT J THERM, 19(4), 1998, pp. 1267-1276
Measurement of the specific heat capacity of molybdenum (standard reference
material) in the temperature range 2000 to 2800 K is described. The method
is based on rapid resistive self-heating of a solid cylindrical specimen f
rom room temperature to the maximum temperature of interest by the passage
of a subsecond-duration electrical current pulse through the specimen with
simultaneous measurement of the pertinent experimental quantities. The expe
rimental quantities yield: the current through the specimen, voltage drop a
cross the specimen, and specimen temperature. The objective of this study i
s to demonstrate the feasibility of performing accurate thermophysical meas
urements where the specimen's true temperature is determined from measureme
nts of surface radiance temperature with a pyrometer and normal spectral em
issivity with a laser polarimeter. This approach of measuring true temperat
ure eliminates the need of having a blackbody configuration for the specime
n. In addition to the specific heat capacity, the normal spectral emissivit
y (at 633 nm) and electrical resistivity of molybdenum in the temperature r
ange from 2000 to 2800 K are presented.