Citation
Vr. Islamgulova et al., Electrochemical synthesis of azodicarboxamide, RUS J AP CH, 71(7), 1998, pp. 1176-1180
Citations number
19
Categorie Soggetti
Chemistry
Journal title
RUSSIAN JOURNAL OF APPLIED CHEMISTRY
ISSN journal
10704272
→ ACNP
Volume
71
Issue
7
Year of publication
1998
Pages
1176 - 1180
Database
ISI
SICI code
1070-4272(199807)71:7<1176:ESOA>2.0.ZU;2-7
Abstract
The possibility was studied of electrochemical synthesis of azodicarboxamid
e by oxidation of hydrazodicarboxamide with anodically generated bromine in
a diaphragmless electrolyzer. An electrolyte composition was found which a
llows performing the process with ORTA anodes. Electrolysis parameters were
determined at which the yield of the target product is as high as 93%. The
possibility was established of recycling the electrolyte solution.