New efficient synthesis of phosphonofluorodithioates ROP(S)(S-)F and theirstructural analogues

Citation
I. Tworowska et W. Dabkowski, New efficient synthesis of phosphonofluorodithioates ROP(S)(S-)F and theirstructural analogues, CHEM COMMUN, (23), 1998, pp. 2611-2612
Citations number
18
Categorie Soggetti
Chemistry
Journal title
CHEMICAL COMMUNICATIONS
ISSN journal
13597345 → ACNP
Issue
23
Year of publication
1998
Pages
2611 - 2612
Database
ISI
SICI code
1359-7345(199812):23<2611:NESOPR>2.0.ZU;2-L
Abstract
The title compounds 3 are formed in very high yield from a one-pot sequenti al reaction of 1,3,2-dithiaphospholane pm derivatives 1, which are transfor med into the corresponding PIV compounds 2 by addition of elemental sulfur and finally into fluoridodithioates 3 by TBAF.