A 50 kV Ga+ focused ion beam was applied for milling submicron Pt-(La0.5Sr0
.5) CoO3-Pb(NbxZryTiz) O-3- (La0.5Sr0.5)CoO3-Pt-based ferroelectric capacit
or heterostructures prepared by pulsed laser and sol-gel deposition techniq
ues. The milling yields were found to be 0.22+/-0.02 mu m(3)/nC for Pb(NbxZ
ryTiz)O-3, 0.3.4+/-0.01 mu m(3)/nC for (La0.5Sr0.5)CoO3, and 0.34 +/- 0.06
mu m(3)/nC for Pt layers. The influence of the ion beam current and its sca
n strategy, as well as depth of milling, on the quality of fabricated struc
tures was' studied. The minimum sizes down to 0.017 mu m(2) for the top ele
ctrode, and 0.04 mu m(2) for the capacitor structures milled to the bottom
electrode were achieved without an additional sacrificial, layer. A scannin
g probe microscopy technique was employed to test the properties of the mil
led capacitor structures. (C) 1998 American Vacuum Society. [S0734-211X(98)
14006-4].