An Al-W-silica integrated circuit interconnect sample was thinned to severa
l mu m and scanned across a 200 nm focal spot of a Fresnel zone plate opera
ting at photon energy of 1573 eV. The experiment was performed on beamline
2-ID-B of the Advanced Photon Source, a third-generation synchrotron facili
ty. Thirteen scanned projections of the sample were acquired over the angul
ar range +/-69.2 degrees. At least 301 X 301 pixels were acquired at each a
ngle with a step size of 77 X 57 nm. A three-dimensional image with an appr
oximate uncertainty of 400 nm was reconstructed from projection data using
a standard algorithm. The two layers of the integrated circuit and the pres
ence of the focused ion beam markers on the surface of the sample are clear
ly shown in the reconstruction. (C) 1999 American Institute of Physics. [S0
003-6951(99)03701-8].