Superior ECD performance through design and application

Citation
Ms. Klee et al., Superior ECD performance through design and application, HRC-J HIGH, 22(1), 1999, pp. 24-28
Citations number
9
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
HRC-JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY
ISSN journal
09356304 → ACNP
Volume
22
Issue
1
Year of publication
1999
Pages
24 - 28
Database
ISI
SICI code
0935-6304(199901)22:1<24:SEPTDA>2.0.ZU;2-E
Abstract
A new ECD, the HP 6890 Series Micro-ECD, was designed to address inherent d eficiencies in classical electron capture detectors (ECD), especially with respect to sensitivity, linearity, dynamic range, and ruggedness. Several n ovel technologies were incorporated in the totally new design and were refi ned through practical testing and user feedback. Validation of the micro-EC D performance was accomplished through side-by-side testing of the Micro-EC D with previous ECDs following US EPA Contract Laboratory Program methods f or pesticides and PCBs, In addition, extensive interviews were conducted wi th early users of the Micro-ECD who also had experience with other designs running a variety of ECD methods. The design and resulting performance impr ovements are described.