The structure and magnetic properties of Nd(Fe, Mo)(12)N-x compounds prepar
ed by mechanical alloying have been studied using x-ray diffraction, transm
ission electron microscopy, and magnetic measurements. After heat treatment
and nitriding, it is found that almost single-phase Nd(Fe, Mo)(12)N-x can
be obtained. Electron microscopy revealed a nanometer grain size of 10-30 n
m and the magnets have a remanence enhancement of approximately 60% of the
saturation. (C) 1998 American Institute of Physics.