Synthesis and X-ray structure of n-phenyl phenylglyoxamide

Citation
S. Boryczka et al., Synthesis and X-ray structure of n-phenyl phenylglyoxamide, J CHEM CRYS, 28(7), 1998, pp. 555-560
Citations number
26
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN journal
10741542 → ACNP
Volume
28
Issue
7
Year of publication
1998
Pages
555 - 560
Database
ISI
SICI code
1074-1542(199807)28:7<555:SAXSON>2.0.ZU;2-Y
Abstract
The title compound (C14H11NO2) is monoclinic with a = 13.579(2), b = 5.297( 1), c = 16.455(2) Angstrom, beta = 98.11(2)degrees, Z = 4, and space group P2(1)/n. The significant structural features lie in the two carbonyl groups of the glyoxamide which are oriented antiperiplanar to each other [-163.6( 3)degrees]. The central bond C(1)-C(2) is 1.545(4) Angstrom. The observed c onformation is stabilized by intramolecular hydrogen bonds.