Em. James et al., Demonstration of atomic resolution Z-contrast imaging by a JEOL JEM-2010F scanning transmission electron microscope, J ELEC MICR, 47(6), 1998, pp. 561-574
The collection of atomic resolution Z-contrast images, using an annular dar
kfield detector, has until recently been exclusively performed using the de
dicated scanning transmission electron microscope (STEM). Here, preliminary
results demonstrate the capability of performing this technique with a 200
kV FEGTEM, featuring a Schottky-emission electron gun. As in the dedicated
STEM, the microscope's spatial resolution limit, for both Z-contrast imagi
ng and chemical micro-analysis experiments, depends on the objective lens s
pherical aberration and the source brightness. Images from a number of mate
rials indicate sub-2 Angstrom Z-contrast resolution. In addition, the instr
ument exhibits probe stability sufficient to observe 1.6 Angstrom lattice f
ringes in coherent convergent beam electron diffraction (CBED) patterns. Us
ing an electron Ronchigram, a spherical aberration coefficient of 0.5 mm ha
s been measured in STEM alignment for one particular pole-piece. Therefore,
higher spatial resolution than that observed here may be possible with a f
urther optimized instrument.