A. Korjakin et al., Comparative study of interlaminar fracture toughness of GFRP with different fiber surface treatments, POLYM COMP, 19(6), 1998, pp. 793-806
This investigation is focused on the influence of glass fiber surface treat
ment on the interlaminar fracture toughness of unidirectional laminates. Th
ree different fiber surface treatments were considered: polyethylene treate
d fibers to get poor adhesion, silane treated fibers to get good bond stren
gth, and industrial fibers without special treatments with the coupling age
nts. The interlaminar fracture behavior of unidirectional glass fiber reinf
orced composites with different fiber surface treatments has been investiga
ted in mode I, mode II, and for the fixed mixed mode I/II ratio 1.33. Doubl
e cantilever beam (DCB), end notched flexure (ENF), and mixed mode flexure
(MMF) specimens were used. The data obtained from these tests were analyzed
by using different analytical approaches and the finite element method. Fo
r the fibers treated with the silane coupling agent, a value about 2.5 time
s higher of mode II interlaminar fracture toughness for crack initiation wa
s obtained in comparison with the polyethylene sized composite. For the com
posite made from the industrial fibers, a value about 2 times higher was ob
tained. Because of extensive fiber bridging and pullout in the composites w
ith poor fiber/matrix adhesion, the results of mode I and mixed mode I/II t
ests did not characterize the interphase quality. In order to determine the
interphase quality, the mode II tests are recommended.