Synthesis and Characterization of 1-chloro-3-methylenecyclopropene

Authors
Litosh, VA Saini, RK Daniels, AD Billups, WE
Citation
Va. Litosh et al., Synthesis and Characterization of 1-chloro-3-methylenecyclopropene, TETRAHEDR L, 40(7), 1999, pp. 1261-1264
Citations number
11
Categorie Soggetti
Chemistry & Analysis","Organic Chemistry/Polymer Science
Journal title
TETRAHEDRON LETTERS
ISSN journal
00404039 → ACNP
Volume
40
Issue
7
Year of publication
1999
Pages
1261 - 1264
Database
ISI
SICI code
0040-4039(19990212)40:7<1261:SACO1>2.0.ZU;2-J
Abstract
1-Chloro-3-methylenecyclopropene was prepared by vacuum gas-solid eliminati on of 2,2-dichloro-1-methylene-3-(trimethylsilyl)cyclopropane over solid ce sium fluoride and characterized by H-1 and C-13 NMR spectroscopy at -103 de grees C. (C) 1999 Elsevier Science Ltd. All rights reserved.