F. Agnes et al., Mesoporous materials synthesized by intercalation of silicate tubes between magadiite layers, APP CATAL A, 176(2), 1999, pp. L153-L158
Synthesis of mesoporous material by pillaring of magadiite with silica was
investigated. For pillaring reactive silica gel with composition characteri
stic for the synthesis of MCM41 was used. The composite samples were charac
terized by XRD, SEM, TG-DTA, IR and BET methods. Increased mechanical stabi
lity of the composite was proven. The acidity of surface OH groups were stu
died by adsorption of pyridine monitored by IR spectroscopy. The results re
vealed the presence of both Bronsted and Lewis acid sites on the aluminium
containing composite. (C) 1999 Elsevier Science B.V. All rights reserved.