NMR study of the hydrolysis and polycondensation of TEOS submitted to the action of ultrasounds

Authors
Moreno, AP Jimenez-Solis, C Esquivias, L Fox, ND
Citation
Ap. Moreno et al., NMR study of the hydrolysis and polycondensation of TEOS submitted to the action of ultrasounds, B S ESP CER, 37(1), 1998, pp. 13-17
Citations number
15
Categorie Soggetti
Material Science & Engineering
Journal title
BOLETIN DE LA SOCIEDAD ESPANOLA DE CERAMICA Y VIDRIO
ISSN journal
03663175 → ACNP
Volume
37
Issue
1
Year of publication
1998
Pages
13 - 17
Database
ISI
SICI code
0366-3175(199801/02)37:1<13:NSOTHA>2.0.ZU;2-1
Abstract
In the present work a study of the gel formation kinetic has been carried o ut by NMR. We show that applying ultrasounds to the mixture TEOS+H2O multip lies concentration of condensed species with regards to the classic obtaine d in alcoholic solution. This difference increases with increasing pH of th e hydrolysis water.