S. Sabolek et E. Babic, DOMAIN-STRUCTURE, PINNING CENTERS AND MAGNETIZATION PROCESSES IN AMORPHOUS AND NANOCRYSTALLINE FE73.5CU1NB3SI15.5B7 RIBBON, Physica status solidi. a, Applied research, 160(1), 1997, pp. 205-214
A detailed analysis of the M-H loops and the corresponding dM/dH versu
s H curves for a Fe73.5Cu1Nb3Si15.5B7 ribbon has been performed for di
fferent stages of successive annealing (T-a less than or equal to 540
degrees C). The application of the model for the influence of the core
current generated fields H-p on the process of magnetization of ferro
magnetic ribbons showed that in the amorphous state (T-a less than or
equal to 300 degrees C) only a fraction of the main (inner) domain str
ucture participates in the process of magnetization. Further annealing
strongly reduces the local anisotropy and the average pinning strengt
h of the domain walls [S-u] which results in a very low coercive field
H-c for 400 degrees C less than or equal to T-a less than or equal to
500 degrees C. Simultaneously, the maximum magnetization M-m becomes
almost equal to the saturation magnetization M-s (approximate to 1.3 T
) already in low magnetizing field (H-0 = 100 A/m). The minimum of H-c
(T-a = 450 degrees C) is associated with the formation of nanocrystal
line Fe3Si grains. High M-m and maximum permeability mu(max) and a low
angle [delta] (between the domain magnetizations and the ribbon axis)
shows that the whole domain structure is very simple in this range of
T-a. Further annealing (T-a > 500 degrees C) increases [S-u] and [del
ta] (which increases H-c) and reduces drastically mu(max) which is con
sistent with the earlier results for similar samples.