R. Lanouette et al., OPTIMIZATION OF AN ALKALINE PEROXIDE INTERSTAGE TREATMENT OF JACK PINE (PINUS-BANKSIANA LAMB) USING A D-OPTIMAL DESIGN, Canadian journal of chemical engineering, 75(1), 1997, pp. 70-78
For many decades, the utilization of jack pine in the pulp and paper i
ndustry has attracted considerable interest but without any major brea
kthrough. However, in the past few years the emergence of new technolo
gies has provided hope for its potential use. One of these technologie
s consists in the addition of hydrogen peroxide within the thermomecha
nical pulping process. To study the influence of numerous process para
meters on the interstage treatment of jack pine and to optimize this c
omplex process, a D-optimal experimental design was conducted. A total
of 7 variables were considered. It was found that to maximize the pro
perties of the fibres and the resulting paper, a temperature of 115 de
grees C with a narrow plate gap at the first refining stage and a high
consistency at the second stage had to prevail. A sodium hydroxide tr
eatment radically improved the fibre bonding properties without affect
ing the tear strength but at the expense of a loss of 4,6 points in IS
O brightness. Validation trials allow to draw some conclusions on the
advantages and shortcomings of this type of experimental design. This
design is efficient, provided sufficient information is available to t
arget likely interactions. Otherwise, a screening design would be requ
ired thus increasing the total cost of the study.