An approach to the determination of platinum-group metals in carbonaceous r
ocks is proposed with due regard to the wide diversity of compounds formed
by platinum-group metals in these rocks. A necessary condition for the corr
ect determination of platinum-group metals is the complete decomposition of
the carbonaceous matter of a rock. At the initial stage of the analysis, t
he decomposition of a sample and the elimination of carbon are achieved by
annealing the samples in an oxygen atmosphere at 60-700 degrees C.