Silicon tetramethoxide was polymerized within a nonionic lyotropic lamellar
phase. After gelation, the birefringence of the sample is preserved and po
larized light optical microscope observations reveal no segregation. High R
esolution Small Angle X-ray Scattering patterns of the gel shows Bragg peak
s characteristic of a layered structure. Freeze fracture experiments on the
lamellar gel show stacks of parallel bilayers. The experimental observatio
ns indicate that the silica is located in the lamellar structure.