Spectrophotometric determination of sulphide using flow injection analysis

Citation
M. Yaqoob et al., Spectrophotometric determination of sulphide using flow injection analysis, J CHEM S P, 20(3), 1998, pp. 214-216
Citations number
10
Categorie Soggetti
Chemistry
Journal title
JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN
ISSN journal
02535106 → ACNP
Volume
20
Issue
3
Year of publication
1998
Pages
214 - 216
Database
ISI
SICI code
0253-5106(199809)20:3<214:SDOSUF>2.0.ZU;2-0
Abstract
A spectrophotometric flow injection procedure for the determination of sulp hide is described. The reaction is based on the reduction of Fe(III) to Fe( II) by sulphide in acidic medium in the presence of 1,10 phenanthroline for ming the orange-red complex [(C12H8N2)(3) Fe](2+) measured at 510 nm. The d etection limit was lower than 1x10(-6) M with sampling rate of 50 h(-1) hav ing a relative standard deviation of 0.96% (n=10).