Crystal structure of N-p-tolyl-4-methyl-5-nitro-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C16H18N2O3, of N-p-tolyl-4-methyl-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C16H19NO and of N-p-tolyl-4,4-dimethyl-5-nitro-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C17H20N2O3

Authors
Hergold-Brundic, A Mestrovic, E Nagl, A Mance, AD Jakopcic, K
Citation
A. Hergold-brundic et al., Crystal structure of N-p-tolyl-4-methyl-5-nitro-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C16H18N2O3, of N-p-tolyl-4-methyl-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C16H19NO and of N-p-tolyl-4,4-dimethyl-5-nitro-3a,4,5,7a-tetrahydro-5,7a-epoxyisoindoline, C17H20N2O3, Z KRIST-NEW, 214(1), 1999, pp. 113-116
Citations number
4
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
ISSN journal
14337266 → ACNP
Volume
214
Issue
1
Year of publication
1999
Pages
113 - 116
Database
ISI
SICI code
1433-7266(1999)214:1<113:CSON>2.0.ZU;2-G
Abstract
C16H18N2O3, monoclinic, P12(1)/c1 (No. 14), a = 15.669(2) Angstrom, b = 6.4 18(1) Angstrom, c = 15.093(3) Angstrom, beta = 113.00(1)degrees, V = 1397.2 Angstrom(3), Z = 4, rho(m) = 1.355 g.cm(-3), R-gt(F) = 0.057, R-w(F) = 0.0 57, T = 293 K. C16H19NO, triclinic, P (1) over bar (No. 2), a = 11.536(2) Angstrom, b = 5. 680(2) Angstrom, c = 10.747(4) Angstrom, alpha = 82.56(3)degrees, beta = 72 .35(3)degrees, gamma = 74.88(2)degrees. V = 646.8 Angstrom(3), Z = 2, rho(m ) 1.234 g.cm(-3), R-gt(F) = 0.049, R-w(F) = 0.069, T = 293 K. C17H20N2O3, monoclinic, P12(1)/c1 (No. 14), a = 13.465(3) Angstrom, b = 7.8 59(1) A, c = 14.819(5) Angstrom, beta = 106.05(2)degrees, V = 1507.1 Angstr om(3) Z = 4, rho(m) = 1.324 g.cm(-3), R-gt(F) = 0.046, R-w(F) = 0.046, T = 293 K.