Nanocomposite films of gold nanoparticles and TiO2 gel have been successful
ly prepared by combination of a surface sol-gel technique and layer-by-laye
r assembly. Thanks to surface hydroxyl groups of gold nanoperticles, gold p
articles were deposited as close-packed monolayers on TiO2 Gel Layers on Ti
O2 gel layers. The resulting nanocomposite contained ca. 50 wt % of gold. M
ultilayer films were successfully prepared by alternate assembly of TiO2 ge
l and gold nanoparticles.