W. Beck et al., Characterization of palladium(II) azide and crystal structure of bis(azido)bis(pyridine)palladium(II) and tetramminepalladium tetraazidopalladate(II), EUR J INORG, (3), 1999, pp. 523-526
Palladium(II) azide (1) was synthesized by reaction of palladium nitrate an
d sodium azide. 1 was characterized by AAS, IR, and N-14-NMR spectroscopy.
Bis(azido)bis(pyridine)palladium(II) (2) and tetramminepalladium tetraazido
palladate(II) (3) were synthesized by a high-yield reaction. Both were char
acterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy.