Crystal structure of 3H-1,2-benzodithiol-3-one 1-oxide

Authors
Behroozi, SJ Barnes, CL Gates, KS
Citation
Sj. Behroozi et al., Crystal structure of 3H-1,2-benzodithiol-3-one 1-oxide, J CHEM CRYS, 28(9), 1998, pp. 689-691
Citations number
15
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN journal
10741542 → ACNP
Volume
28
Issue
9
Year of publication
1998
Pages
689 - 691
Database
ISI
SICI code
1074-1542(199809)28:9<689:CSO31>2.0.ZU;2-#
Abstract
The compound 3H-1,2-benzodithiol-3-one 1-oxide (2) has proven useful in mod eling the reactivity of the novel antitumor antibiotic leinamycin (1). The crystal structure of this unusual sulfur heterocycle is reported here. The molecule crystallizes in the P-1 space group with cell parameters a = 7.168 (4), b = 7.670(3), c = 7.922(3)Angstrom, alpha = 68.34(4), beta = 83.86(3), gamma = 65.50(3),degrees and U = 367.8 Angstrom(3).